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Nuclear magnetic resonance (NMR) spectroscopy NMR samples (600 L final volume) were prepared in 5 mm NMR tubes (Sigma-Aldrich) by dissolving FeS samples in the respective buffer supplemented with 10% D 2 O (v/v) and 0.001% DSS (w/v) as an internal chemical shift reference

Bergman RN, Kim SP, Hsu IR, Catalano KJ, Chiu JD, Kabir M, Richey JM, Ader M: Abdominal obesity: role in the pathophysiology of metabolic disease and cardiovascular risk

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